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         "number": "22","pages": "4510--4520","abstract": "Isomeric dichalcogenides [Me2NCH(Me)CH2E]2 [(N$\\cap$E**)2] and [Me2NCH2CH(Me)E]2 [(N$\\cap$E*)2] (E = S, Se, Te) were obtained by the reactions of NaSH or M'2E2 (M' = Na or K) with Me2NCH2CHMeCl.  The former reaction affords mainly (N$\\cap$E**)2 (E = S) while from the latter mixts. of (N$\\cap$E**)2 and (N$\\cap$E*)2 [referred to as (N$\\cap$E)2, E = S, Se, Te] were isolated, the ratios in the mixts. depending on the chalcogen.  Reactions of (N$\\cap$E)Na with [M2Cl2(m-Cl)2(PR3)2] gave [MCl(N$\\cap$E)(PR3)] (M = Pd or Pt).  These chiral, mixed-ligand complexes were characterized by elemental anal., IR, UV/visible and NMR (1H, 13C, 31P, 77Se, 125Te, 195Pt) spectroscopy, and, in part, by x-ray structure anal.  The complexes display a typical pattern of mutually trans-oriented neutral (P and N) and anionic (Cl and E) donor atoms in an approx. square-planar environment.  In contrast to the Pt(II) analogs, the x-ray structures of [PdCl(N$\\cap$E)(PMePh2)] (E = S or Se) revealed both a conformational isomerism of the five-membered chelate ring and, for Se, the co-crystn. of complexes with both the N$\\cap$E* and N$\\cap$E** isomeric ligands.  The thermal behavior of some complexes was studied. [on SciFinder(R)]",
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         "number": "22","pages": "4510--4520","abstract": "Isomeric dichalcogenides [Me2NCH(Me)CH2E]2 [(N$\\cap$E**)2] and [Me2NCH2CH(Me)E]2 [(N$\\cap$E*)2] (E = S, Se, Te) were obtained by the reactions of NaSH or M'2E2 (M' = Na or K) with Me2NCH2CHMeCl.  The former reaction affords mainly (N$\\cap$E**)2 (E = S) while from the latter mixts. of (N$\\cap$E**)2 and (N$\\cap$E*)2 [referred to as (N$\\cap$E)2, E = S, Se, Te] were isolated, the ratios in the mixts. depending on the chalcogen.  Reactions of (N$\\cap$E)Na with [M2Cl2(m-Cl)2(PR3)2] gave [MCl(N$\\cap$E)(PR3)] (M = Pd or Pt).  These chiral, mixed-ligand complexes were characterized by elemental anal., IR, UV/visible and NMR (1H, 13C, 31P, 77Se, 125Te, 195Pt) spectroscopy, and, in part, by x-ray structure anal.  The complexes display a typical pattern of mutually trans-oriented neutral (P and N) and anionic (Cl and E) donor atoms in an approx. square-planar environment.  In contrast to the Pt(II) analogs, the x-ray structures of [PdCl(N$\\cap$E)(PMePh2)] (E = S or Se) revealed both a conformational isomerism of the five-membered chelate ring and, for Se, the co-crystn. of complexes with both the N$\\cap$E* and N$\\cap$E** isomeric ligands.  The thermal behavior of some complexes was studied. [on SciFinder(R)]",
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