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         "id"   : "https://puma.ub.uni-stuttgart.de/bibtex/28595b6a86b9e7f051cfe930f8c8dbeda/ipappwiedmann",         
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         "id"   : "https://puma.ub.uni-stuttgart.de/bibtex/2fc43475cc109889bb85956b19cb03e2e/huebleriac",         
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         "label" : "Complex Series [Ru(tpy)(dpk)(X)]n+ (tpy = 2,2': 6',2''-Terpyridine; dpk = 2,2'-Dipyridyl Ketone; X = Cl-, CH3CN, NO2-, NO+, NO.bul., NO-): Substitution and Electron Transfer, Structure, and Spectroscopy",
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         "volume": "44","number": "17","pages": "6092--6099","abstract": "The complex framework [Ru(tpy)(dpk)]2+ (tpy = 2,2':6',2''-terpyridine, dpk = 2,2'-dipyridyl ketone) was used to study the generation and reactivity of the nitrosyl complex [Ru(tpy)(dpk)(NO)]3+ ([4]3+).  Stepwise conversion of the chloro complex [Ru(tpy)(dpk)(Cl)]+ ([1]+) via [Ru(tpy)(dpk)(MeCN)]2+ ([2]2+) and the nitro compd. [Ru(tpy)(dpk)(NO2)]+ ([3]+) yielded [4]3+; all four complexes were structurally characterized as perchlorates.  Electrochem. oxidn. and redn. were studied as a function of the monodentate ligand as were the IR and UV-visible spectroscopic responses (absorption/emission).  The kinetics of the nitroso-to-nitro conversion [4]3+/[3]+ in aq. environment were also studied.  Two-step redn. of [4]3+ was monitored via EPR, UV-visible, and IR (n(NO), n(CO)) spectroelectrochem. to confirm the RuNO7 configuration of [4]2+ and to exhibit a relatively intense band at 505 nm for [4]+, attributed to a ligand-to-ligand transition originating from bound NO-. [on SciFinder(R)]",
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         "label" : "Formation, reactivity, and photorelease of metal bound nitrosyl in [Ru(trpy)(L)(NO)]n+ (trpy = 2,2':6',2''-terpyridine, L = 2-phenylimidazo[4,5-f]1,10-phenanthroline)",
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         "author": [ 
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            	{"first" : "Somnath",	"last" : "Maji"},
            	{"first" : "Biprajit",	"last" : "Sarkar"},
            	{"first" : "Malay",	"last" : "Patra"},
            	{"first" : "Atanu Kumar",	"last" : "Das"},
            	{"first" : "Shaikh M.",	"last" : "Mobin"},
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            	{"first" : "Goutam Kumar.",	"last" : "Lahiri"}
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         "volume": "47","number": "8","pages": "3218--3227","abstract": "Nitrosyl complexes with Ru-NO6 and Ru-NO7 configurations were isolated in the framework of [Ru(trpy)(L)(NO)]n+ [trpy = 2,2':6',2''-terpyridine, L = 2-phenylimidazo[4,5-f]1,10-phenanthroline] as the perchlorate salts [4](ClO4)3 and [4](ClO4)2, resp.  Single crystals of protonated material [4-H+](ClO4)4·2H2O reveal a Ru-N-O bond angle of 176.1(7)° and triply bonded N-O with a 1.127(9) \\AA bond length.  Structures were also detd. for precursor compds. of [4]3+ as [Ru(trpy)(L)(Cl)](ClO4)·4.5H2O and [Ru(trpy)(L-H)(CH3CN)](ClO4)3·H2O.  In agreement with largely NO centered redn., a sizable shift in n(NO) frequency was obsd. on moving from [4]3+ (1953 cm-1) to [4]2+ (1654 cm-1).  The RuII-NO.bul. in isolated or electrogenerated [4]2+ exhibits an EPR spectrum with g1 = 2.020, g2 = 1.995, and g3 = 1.884 in CH3CN at 110 K, reflecting partial metal contribution to the singly occupied MO (SOMO); 14N (NO) hyperfine splitting (A2 = 30 G) was also obsd.  The plot of n(NO) vs. E°(RuNO6 $\\rightarrow$ RuNO7) for 12 analogous complexes [Ru(trpy)(L')(NO)]n+ exhibits a linear trend.  The electrophilic Ru-NO+ species [4]3+ is transformed to the corresponding Ru-NO2- system in the presence of OH- with k = 2.02 $\\times$ 10-4 s-1 at 303 K.  In the presence of a steady flow of dioxygen gas, the RuII-NO.bul. state in [4]2+ oxidizes to [4]3+ through an associatively activated pathway (DSdpl = -190.4 J K-1 M-1) with a rate const. (k [s-1]) of 5.33 $\\times$ 10-3.  On irradn. with light (Xe lamp), the acetonitrile soln. of paramagnetic [Ru(trpy)(L)(NO)]2+ ([4]2+) undergoes facile photorelease of NO (kNO = 2.0 $\\times$ 10-1 min-1 and t1/2 $\\approx$ 3.5 min) with the concomitant formation of the solvate [RuII(trpy)(L)(CH3CN)]2+ [2']2+.  The photoreleased NO can be trapped as an Mb-NO adduct. [on SciFinder(R)]",
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         "author": [ 
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         "label" : "Sites of Electron Transfer Reactivity in Organometallic Compounds",
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         "volume": "2020","number": "11-12","pages": "875--878","abstract": "A review.  Three essentially different sites are identified for redox activity in organometallic compds.: The metal, the organometallic (C-bonded) ligand(s), and potentially non-innocent co-ligands.  Typical reactivity patterns resulting from either of these alternatives will be pointed out by means of representative examples, possibly involving unusual metal oxidn. states, carbon-centered radicals, or ligand redox systems. [on SciFinder(R)]",
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         "label" : "Formation, reactivity, and photorelease of metal bound nitrosyl in [Ru(trpy)(L)(NO)]n+ (trpy = 2,2':6',2''-terpyridine, L = 2-phenylimidazo[4,5-f]1,10-phenanthroline)",
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            	{"first" : "Biprajit",	"last" : "Sarkar"},
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            	{"first" : "Atanu Kumar",	"last" : "Das"},
            	{"first" : "Shaikh M.",	"last" : "Mobin"},
            	{"first" : "Wolfgang",	"last" : "Kaim"},
            	{"first" : "Goutam Kumar.",	"last" : "Lahiri"}
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         "volume": "47","number": "8","pages": "3218--3227","abstract": "Nitrosyl complexes with Ru-NO6 and Ru-NO7 configurations were isolated in the framework of [Ru(trpy)(L)(NO)]n+ [trpy = 2,2':6',2''-terpyridine, L = 2-phenylimidazo[4,5-f]1,10-phenanthroline] as the perchlorate salts [4](ClO4)3 and [4](ClO4)2, resp.  Single crystals of protonated material [4-H+](ClO4)4·2H2O reveal a Ru-N-O bond angle of 176.1(7)° and triply bonded N-O with a 1.127(9) \\AA bond length.  Structures were also detd. for precursor compds. of [4]3+ as [Ru(trpy)(L)(Cl)](ClO4)·4.5H2O and [Ru(trpy)(L-H)(CH3CN)](ClO4)3·H2O.  In agreement with largely NO centered redn., a sizable shift in n(NO) frequency was obsd. on moving from [4]3+ (1953 cm-1) to [4]2+ (1654 cm-1).  The RuII-NO.bul. in isolated or electrogenerated [4]2+ exhibits an EPR spectrum with g1 = 2.020, g2 = 1.995, and g3 = 1.884 in CH3CN at 110 K, reflecting partial metal contribution to the singly occupied MO (SOMO); 14N (NO) hyperfine splitting (A2 = 30 G) was also obsd.  The plot of n(NO) vs. E°(RuNO6 $\\rightarrow$ RuNO7) for 12 analogous complexes [Ru(trpy)(L')(NO)]n+ exhibits a linear trend.  The electrophilic Ru-NO+ species [4]3+ is transformed to the corresponding Ru-NO2- system in the presence of OH- with k = 2.02 $\\times$ 10-4 s-1 at 303 K.  In the presence of a steady flow of dioxygen gas, the RuII-NO.bul. state in [4]2+ oxidizes to [4]3+ through an associatively activated pathway (DSdpl = -190.4 J K-1 M-1) with a rate const. (k [s-1]) of 5.33 $\\times$ 10-3.  On irradn. with light (Xe lamp), the acetonitrile soln. of paramagnetic [Ru(trpy)(L)(NO)]2+ ([4]2+) undergoes facile photorelease of NO (kNO = 2.0 $\\times$ 10-1 min-1 and t1/2 $\\approx$ 3.5 min) with the concomitant formation of the solvate [RuII(trpy)(L)(CH3CN)]2+ [2']2+.  The photoreleased NO can be trapped as an Mb-NO adduct. [on SciFinder(R)]",
         "issn" : "0020-1669",
         
         "doi" : "10.1021/ic702160w",
         
         "bibtexKey": "Maji.2008"

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         "volume": "44","number": "17","pages": "6092--6099","abstract": "The complex framework [Ru(tpy)(dpk)]2+ (tpy = 2,2':6',2''-terpyridine, dpk = 2,2'-dipyridyl ketone) was used to study the generation and reactivity of the nitrosyl complex [Ru(tpy)(dpk)(NO)]3+ ([4]3+).  Stepwise conversion of the chloro complex [Ru(tpy)(dpk)(Cl)]+ ([1]+) via [Ru(tpy)(dpk)(MeCN)]2+ ([2]2+) and the nitro compd. [Ru(tpy)(dpk)(NO2)]+ ([3]+) yielded [4]3+; all four complexes were structurally characterized as perchlorates.  Electrochem. oxidn. and redn. were studied as a function of the monodentate ligand as were the IR and UV-visible spectroscopic responses (absorption/emission).  The kinetics of the nitroso-to-nitro conversion [4]3+/[3]+ in aq. environment were also studied.  Two-step redn. of [4]3+ was monitored via EPR, UV-visible, and IR (n(NO), n(CO)) spectroelectrochem. to confirm the RuNO7 configuration of [4]2+ and to exhibit a relatively intense band at 505 nm for [4]+, attributed to a ligand-to-ligand transition originating from bound NO-. [on SciFinder(R)]",
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            	{"first" : "Sanjib",	"last" : "Kar"},
            	{"first" : "Shaikh M.",	"last" : "Mobin"},
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            	{"first" : "Goutam Kumar.",	"last" : "Lahiri"}
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         "volume": "44","number": "17","pages": "6092--6099","abstract": "The complex framework [Ru(tpy)(dpk)]2+ (tpy = 2,2':6',2''-terpyridine, dpk = 2,2'-dipyridyl ketone) was used to study the generation and reactivity of the nitrosyl complex [Ru(tpy)(dpk)(NO)]3+ ([4]3+).  Stepwise conversion of the chloro complex [Ru(tpy)(dpk)(Cl)]+ ([1]+) via [Ru(tpy)(dpk)(MeCN)]2+ ([2]2+) and the nitro compd. [Ru(tpy)(dpk)(NO2)]+ ([3]+) yielded [4]3+; all four complexes were structurally characterized as perchlorates.  Electrochem. oxidn. and redn. were studied as a function of the monodentate ligand as were the IR and UV-visible spectroscopic responses (absorption/emission).  The kinetics of the nitroso-to-nitro conversion [4]3+/[3]+ in aq. environment were also studied.  Two-step redn. of [4]3+ was monitored via EPR, UV-visible, and IR (n(NO), n(CO)) spectroelectrochem. to confirm the RuNO7 configuration of [4]2+ and to exhibit a relatively intense band at 505 nm for [4]+, attributed to a ligand-to-ligand transition originating from bound NO-. [on SciFinder(R)]",
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